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Validation in Chemical Measurement
Validationofmeasurementmethodshasbeenusedforavery ciated measurement uncertainty? The answer must be: no. longtimeinchemistry. Itismostlybasedontheexamination Therecanneverbeamechanismorrecipeforproducing - of a measurement procedure for its characteristics such as tomatically valid results because...
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| Auteurs principaux : | , , |
|---|---|
| Format : | Livre |
| Langue : | anglais |
| Titre complet : | Validation in Chemical Measurement / edited by Paul Bièvre, Helmut Günzler. |
| Publié : |
Berlin, Heidelberg :
Springer Berlin Heidelberg
, 2005 Cham : Springer Nature |
| Accès en ligne : |
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| Documents associés : | Autre format:
Validation in Chemical Measurement Autre format: Validation in Chemical Measurement Autre format: Validation in Chemical Measurement |
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| 200 | 1 | |a Validation in Chemical Measurement |f edited by Paul Bièvre, Helmut Günzler. | |
| 214 | 0 | |a Berlin, Heidelberg |c Springer Berlin Heidelberg | |
| 214 | 2 | |a Cham |c Springer Nature |d 2005 | |
| 330 | |a Validationofmeasurementmethodshasbeenusedforavery ciated measurement uncertainty? The answer must be: no. longtimeinchemistry. Itismostlybasedontheexamination Therecanneverbeamechanismorrecipeforproducing - of a measurement procedure for its characteristics such as tomatically valid results because one can never eliminate precision, accuracy, selectivity, sensitivity, repeatability, re- theskills,theroleandtheresponsibilityoftheanalyst. producibility,detectionlimit,quanti?cationlimitandmore. ISO 9000:2000, item 3. 8. 5 de?nes validation as con?r- When focussing on quality comparability and reliability mation by examination and provision of objective evidence in chemical measurement, the ?elds of interest to this Jour- that the requirements for an intended use are ful?lled . The nal, one stumbles into various interpretations of the term revised edition of the VIM ( VIM3 ), is likely to ?ne-tune validation. It is one more example of a term which is used thisde?nitionoftheconcept validation tobe con?rmation sometimes very consistently, sometimes very loosely or in- through examination of a given item and provision of - deed ambiguously. Since the term is very common in the jective evidence that it ful?lls the requirements for a stated chemical community, it is important that its meaning be intendeduse . nd clear. Turning to the 2 edition of the International Vo- Lookingatsimplepractice, manypeoplearelookingfor cabulary of Basic and General terms in Metrology (VIM) aformaldecisionthatagivenmeasurementmethod automat- (1993), surprisingly we do not ?nd a de?nition. Webster s ically gives them valid i. e. reliable results. One wonders Dictionary of the English language (1992) tells us that val- what this has to do with stated intended use . Reliab- idation is making or being made valid . Obviously valida- ity clearly is a property of a measurement result | ||
| 359 | 1 | |a Bioanalytical method validation and its implications for forensic and clinical toxicology A review -- Validation of a computer program for atomic absorption analysis -- Instrumental validation in capillary electrophoresis and checkpoints for method validation -- Qualification and validation of software and computer systems in laboratories -- Clinical reference materials for the validation of the performance of photometric systems used for clinical analyses -- Measurement uncertainty and its implications for collaborative study method validation and method performance parameters -- Qualification and validation of software and computer systems in laboratories -- Qualification and validation of software and computer systems in laboratories -- Qualification and validation of software and computer systems in laboratories -- Analytical validation in practice at a quality control laboratory in the Japanese pharmaceutical industry -- Validation of the uncertainty evaluation for the determination of metals in solid samples by atomic spectrometry -- Validation requirements for chemical methods in quantitative analysis horses for courses? -- Validation criteria for developing ion-selective membrane electrodes for analysis of pharmaceuticals -- Is the estimation of measurement uncertainty a viable alternative to validation? -- Validation of an HPLC method for the determination of p-dichlorobenzene and naphthalene in mothrepellents -- The evaluation of measurement uncertainty from method validation studies -- The evaluation of measurement uncertainty from method validation studies -- Automated ion-selective measurement of lithium in serum. A practical approach to result-level verification in a two-way method validation -- Determination of hydrocarbons in water interlaboratory methodvalidation before routine monitoring -- Interlaboratory quality audit program for potable water assessment of method validation done on inductively coupled plasma atomic emission spectrometer (ICP-AES) -- A need for clearer terminology and guidance in the role of reference materials in method development and validation -- Validation of salt spray corrosion test -- Method validation and reference materials -- Method validation of modern analytical techniques -- Validation of test methods -- Marketing Valid Analytical Measurement -- Analytical procedure in terms of measurement (quality) assurance -- Flexibilization of the scope of accreditation: an important asset for food and water microbiology laboratories -- Different approaches to legal requirements on validation of test methods for official control of foodstuffs and of veterinary drug residues and element contaminants in the EC -- Methods validation: AOAC s three validation systems -- Observing validation, uncertainty determination and traceability in developing Nordtest test methods. | |
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